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Syrian government forces have been accused of dropping barrel bombs containing chlorine from helicopters on a suburb of Aleppo, injuring 80 people.
Volunteer emergency workers say people suffered breathing difficulties after an attack on the Sukari area.
The reports could not be independently verified. AUN-led investigation in August found the government had used chlorine on at least two occasions.
The Syrian government has always denied using chemical weapons.
It comes as Syrian opposition leaders prepare to meet in London on Wednesday to launch a new plan for a political transition to try to end the conflict.
The opposition’s main political group, the High Negotiations Committee, will be hosted by UK Foreign Minister Boris Johnson and foreign ministers from the Friends of Syria group will attend.
Saudi Foreign Minister Adel al-Jubeir told the BBC that he still believed in a political solution to the conflict, and that Mr Assad was not in a “position of advantage or victory”, despite his forces’ recent advances.
“But if Bashar al-Assad continues to be obstinate and continues to drag his feet and continues to refuse to engage seriously, then obviously there will have to be a Plan B which will involve more stepped up military activity,” he said.
Distressed children
Ibrahem Alhaj, a Syrian Civil Defence rescue worker, said he had reached the scene of the Aleppo attack shortly after a helicopter dropped barrels containing what he said were four chlorine cylinders on Tuesday.
Syrian Civil Defence, a volunteer emergency response team that operates in opposition-held areas, posted video on its Facebook page showing distressed children using oxygen masks to breathe.
Images taken by the rescuers show civilians with breathing masks in an unidentified local hospital
Children with breathing difficulties were pictured being treatedThe group accused the government of another chlorine attack in August.
Russia, an ally of the Syrian government, has accused rebels of firing shells containing “toxic gas” at government-held areas in Aleppo.
Chlorine is a common industrial chemical, but its use in weapons is banned by the Chemical Weapons Convention.
Brutal fighting
The UN said on Tuesday that a brief period of relief early this year for civilians caught up in the war in Syria had been replaced by an even more brutal resumption in fighting.
In its 12th report on Syria, it said the cessation of hostilities in February had allowed some towns to receive their first aid in years but it only lasted a few weeks.
Aleppo has been repeatedly targeted by government forces, activists say, as they try to recapture parts of the cityThe report says 600,000 Syrians now live under siege with a further 300,000 trapped in the city of Aleppo.
On Sunday, Syrian government forces were reported to have recaptured parts of Aleppo city which were lost to rebels last month, placing rebel-held districts in the city’s east once again under siege.
Monitors said government troops had recaptured two military academy sites in the Ramouseh district south of the city and severed a recently established rebel supply line.
BBC